Synthesis of Hydroxyapatite from Budu Waste by Calcination Method

Document Type : Research Article

Authors

1 Chemistry Program, Faculty of Science Technology and Agriculture, Yala Rajabhat University, Yala, THAILAND

2 Chemistry Department, Faculty of Mathematics and Natural Science, Universitas Negeri Malang (UM), Malang, INDONESIA

3 Division of Physical Science, Faculty of Science, Prince of Songkla University, Hat Yai, Songkhla, THAILAND

4 Biology Program, Faculty of Science Technology and Agriculture, Yala Rajabhat University, Yala, THAILAND

5 The Halal Science Center, Chulalongkorn University, Bangkok, THAILAND

Abstract

Fish bones contain high calcium, which makes them a good raw material for the preparation of calcium hydroxyapatite (HAp). HAp is usually prepared from fresh fish bones because it has low impurity but there are many waste fish bones from food processing. In this work, HAp was synthesized from Budu waste by maceration process and calcination. Obtained products were characterized by X-ray diffraction (XRD), Fourier transform spectroscopy (FT-IR), and thermal analysis. When the calcination was higher than 600 °C, the product showed a mixture of hydroxyapatite [Ca5(PO4)3OH] as a major phase and merrillite [Ca9MgNa(PO4)7] as a minor phase. The amount of merrillite was increased with an increase in calcination temperature.

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Main Subjects

References

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Iranian Journal of Chemistry and Chemical Engineering
Volume 41, Issue 12 - Serial Number 122
December 2022
Pages 4203-4212

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